COMPARISON OF THE THIXOTROPIC PROPERTIES OF DIFFERENT COMPOSITE MATERIALS FOR BONDING FIXED ORTHODONTIC APPLIANCES DURING EXPERIMENTAL BRACKET PLACEMENT

Authors

DOI:

https://doi.org/10.32782/2786-7684/2026-2-10

Keywords:

dentistry, orthodontic treatment, bracket system, composite materials, drift effect

Abstract

Introduction. The use of fixed orthodontic appliances for the treatment of various malocclusions is a widely applied therapeutic approach in modern dental practice. The application of specialized composite materials for bonding bracket systems to the tooth surface is consequently a routine procedure in clinical dentistry. The phenomenon of uncontrolled flow of orthodontic composites during bracket placement should be considered a key rheological factor that determines the quality of adhesion and the accuracy of orthodontic appliance positioning. The aim of the study was to compare, under experimental conditions, the thixotropic properties of several contemporary orthodontic light-cured composite materials based on the level of bracket “drift effect.” Methodology and methods of the study. Metal brackets (attachments) were temporarily bonded to an organic glass plate using nonpolymerized materials: «JenOrtho», «GC Ortho Connect», «Orthocem», «Biofix», «Enlight», and BracePaste, with six samples per each material. The plates with bonded brackets were positioned vertically and maintained at 37.0 °C for 30 minutes in a thermostat. The thixotropic properties of the materials were assessed based on the degree of secondary bracket displacement (“drift effect”). Summary of the primary study material. The analysis of secondary bracket displacement (“drift effect”) showed that most materials did not exhibit measurable displacement, while only two did. «GC Ortho Connect» demonstrated a statistically significantly higher level of secondary displacement compared to all other composite materials (p < 0.001). «Orthocem» also showed a statistically significant difference compared to the groups without displacement (p < 0.05). For brackets bonded with Biofix, where only minimal displacement was observed, no statistically significant differences were identified. Conclusions. The highest level of displacement was observed for «GC Ortho Connect», whereas «JenOrtho», «Enlight», and «BracePaste» demonstrated complete positional stability. The type of material accounts for the majority of variability in the observed outcomes, highlighting its key role in ensuring the accuracy of bracket fixation.

References

Mandall NA, Millett DT, Mattick CR, Hickman J, Worthington HV, Macfarlane TV. Orthodontic adhesives: a systematic review. J Orthod. 2002;29(3):205-10; discussion 195. doi: 10.1093/ortho/29.3.205.

Thiara S, Sood S, Mahajan M, Negi S, Negi KS, Chainta D, Negi N. Orthodontic bonding in transition: Materials, techniques, and clinical applications. IP Indian Journal of Orthodontics and Dentofacial Research. 2026;12(1):6–13. doi: 10.18231/j.ijodr.13185.1763549759

Altmann AS, Degrazia FW, Celeste RK, Leitune VC, Samuel SM, Collares FM. Orthodontic bracket bonding without previous adhesive priming: A meta-regression analysis. Angle Orthod. 2016;86(3):391-8. doi: 10.2319/041615-255.1.

Vicente A, Bravo LA, Romero M, Ortiz AJ, Canteras M. A comparison of the shear bond strength of a resin cement and two orthodontic resin adhesive systems. Angle Orthod. 2005;75(1):109-13. doi: 10.1043/0003-3219(2005)075<0109:ACOTSB>2.0.CO;2.

Abuljadayel R. Effect of bioactive adhesives on shear bond strength at the enamel-orthodontic bracket interface. J Pioneering Med Sci. 2025;14(S01):26–33. doi:10.47310/jpms202514S0105

Bhuvaneswaran T, Vimala G, Rao GU, Anbarasu P. Comparative Evaluation of orthodontic bonding systems for ceramic brackets on zirconia crowns: A shear Bond Strength and Adhesive remnant Index study. The Journal of Indian Orthodontic Society. 2024;59(1):62–8. doi: 10.1177/03015742241275353

Jain D, Chopra SS, Thakur VK, Sewda SK. Comparative evaluation of bonding failure rate with two light cure orthodontic adhesives: a cross-arch split-mouth prospective study. Dental Press J Orthod. 2025;30(2):e2524214. doi: 10.1590/2177-6709.30.2.e2524214.oar.

Cramer NB, Stansbury JW, Bowman CN. Recent advances and developments in composite dental restorative materials. J Dent Res. 2011;90(4):402-16. doi: 10.1177/0022034510381263.

Ferracane JL. A Historical Perspective on Dental Composite Restorative Materials. J Funct Biomater. 2024;15(7):173. doi: 10.3390/jfb15070173.

Jeconias N, Fischer P, Tauböck TT. Viscosity-Dependent Shrinkage Behavior of Flowable Resin Composites. Polymers (Basel). 2025;17(24):3292. doi: 10.3390/polym17243292.

Lee JH, Um CM, Lee IB. Rheological properties of resin composites according to variations in monomer and filler composition. Dent Mater. 2006;22(6):515-26. doi: 10.1016/j.dental.2005.05.008.

Papadogiannis D, Iliadi A, Bradley TG, Silikas N, Eliades G, Eliades T. Viscoelastic properties of orthodontic adhesives used for lingual fixed retainer bonding. Dent Mater. 2017;33(1):e22–e27. doi:10.1016/j.dental.2016.09.041

Scribante A, Vallittu PK, Özcan M. Fiber-reinforced composites for dental applications. Biomed Res Int. 2018;2018:4734986. doi:10.1155/2018/4734986.

Szczesio-Wlodarczyk A, Garoushi S, Vallittu P, Bociong K, Lassila L. Polymerization shrinkage stress of contemporary dental composites: Comparison of two measurement methods. Dental Materials Journal. 2024;43(2):155–63. doi: 10.4012/dmj.2023-192.

Condò R, Mampieri G, Cioffi A, Pirelli P, Giancotti A, Maiolo L, Maita F, Convertino A, Lucarini I, Notargiacomo A, Rau JV, Fosca M, Marzo G. Relationship between Reflectivity, Chemical Composition and Mechanical Behaviour of Orthodontic Bonding Nanofiller Resin Materials: A Proposal of an Alternative Method of Investigation. Applied Sciences. 2022;12(24):12538. doi: 10.3390/app122412538

Namura Y, Takamizawa T, Uchida Y, Inaba M, Noma D, Takemoto T, Miyazaki M, Motoyoshi M. Effects of composition on the hardness of orthodontic adhesives. J Oral Sci. 2020;62(1):48-51. doi: 10.2334/josnusd.19-0035.

Chanachai S, Chaichana W, Insee K, Benjakul S, Aupaphong V, Panpisut P. Physical/Mechanical and Antibacterial Properties of Orthodontic Adhesives Containing Calcium Phosphate and Nisin. J Funct Biomater. 2021;12(4):73. doi: 10.3390/jfb12040073.

Owens SE Jr, Miller BH. A comparison of shear bond strengths of three visible light-cured orthodontic adhesives. Angle Orthod. 2000;70(5):352-6. doi: 10.1043/0003-3219(2000)070<0352:ACOSBS>2.0.CO;2.

Schneider LF. Light and viscosity effects on curing potential of composites. OHI-S. 2023. URL: https://ohi-s.com/articles-videos/light-and-viscosity-efects-on-the-curing-potential-of-bulk-fll-composites-placed-in-deep-cavities/

Mirzakouchaki B, Kimyai S, Hydari M, Shahrbaf S, Mirzakouchaki-Boroujeni P. Effect of self-etching primer/adhesive and conventional bonding on the shear bond strength in metallic and ceramic brackets. Medicina Oral, Patología Oral Y Cirugía Bucal. 2012;17(1):e164–70. doi: 10.4317/medoral.17024

Sharma S, Tandon P, Nagar A, Singh GP, Singh A, Chugh VK. A comparison of shear bond strength of orthodontic brackets bonded with four different orthodontic adhesives. J Orthod Sci. 2014;3(2):29-33. doi: 10.4103/2278-0203.132892.

Staehle HJ, Sekundo C. 75 Years Ago: Discovery of Resin Adhesion to Acid-etched Enamel – A Comparison of the 1949 and 1955 Methods. J Adhes Dent. 2024;26:87-92. doi: 10.3290/j.jad.b5057135.

Pseiner BC, Freudenthaler J, Jonke E, Bantleon HP. Shear bond strength of fluoride-releasing orthodontic bonding and composite materials. Eur J Orthod. 2010;32(3):268-73. doi: 10.1093/ejo/cjp116.

Published

2026-05-30

Issue

Section

DENTISTRY